Environmental Soil/Biosolids

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Land Application Packages

Package II: Total Solids, Ammonia N, Nitrate-N, Total N, Phosphorus, Potassium, Lead, Zinc, Copper, Nickel, Cadmium, Arsenic, Mercury, Molybdenum, Selenium
Package IIIA: (MI & OH) Total Solids, Ammonia-N, Nitrate-N, Total N, Phosphorus, Potassium, Lead, Zinc, Copper, Nickel, Cadmium, Arsenic, Mercury, Molybdenum, Selenium, pH
Package IIIB: (IL) Total Solids, Ammonia-N, Nitrate-N, Total N, Phosphorus, Potassium, Lead, Zinc, Copper, Nickel, Cadmium, Arsenic, Mercury, Molybdenum, Selenium, pH, Chromium, Manganese, Volatile Solids
Package IV: Nutrients Total Solids, Ammonia N, Nitrate-N, Total N, Phosphorus, Potassium
Package V: Lime Sludge Total Solids, PCB's, Lead, Zinc, Copper, Nickel, Cadmium, Arsenic, Mercury, Molybdenum, Selenium, CCE, Sieve Analysis: 8, 20, 60, 100 Mesh
Package VI: 503 Metals Total Solids, Lead, Zinc, Copper, Nickel, Cadmium, Arsenic, Mercury, Molybdenum, Selenium
Class A Fecal Coliform Package MPN, 7 individual samples, includes % Solids
Class B Fecal Coliform Package MPN, 7 individual samples, includes % Solids
Class B Fecal Coliform Package CFU, 7 individual samples, includes % Solids

Organics (GC-GC/MS)

Organics (GC-GC/MS): Method
Acid Extractables SW846-8270C
Base Neutral Extractables SW846-8270C
PCB' s SW846-8082
Pesticides SW846-8081A
Volatiles SW846-8260B

Individual Non-Metals

Non-Metals Method
Bacteria
Coliform, Fecal (CFU/g dry) - Class B*
SM(20th)-9222D
Coliform, Fecal (MPN/g dry)-Class A*
SM(20th)-9221E
Coliform, Fecal (MPN/g dry)-Class B*
 SM(20th)-9221E
Heterotrophic Plate Count (CFU/g dry)*
 SM(20th)-9215B
Salmonella (MPN/g dry)*
 SM(20th)-9260B
Total Bacteria (CFU/g)*
 SM(20th)-9215C
BOD, 5-Day** SM(20th)-5210B
Chloride SM(20th)-4500 Cl- G
Chromium Hexavalent SW846-3060A
Cyanide, Amenable SW846-9010C/9012B
Cyanide, Reactive SW846--7.3.3.2
Cyanide, Total SW846-9010C/9012B
Fluoride SW846-9214
Nitrogen, Ammonia SM(20th)-4500-NH3 B/NH3 C
Nitrogen, Nitrate EPA-353.2 Mod
Nitrogen, Nitrite EPA-353.2 Mod
Nitrogen, Nitrate + Nitrite EPA-353.2 Mod
Nitrogen, Organic Calculation (TKN - NH3-N)
Nitrogen, Total Kjeldahl SM(20th)-4500-Norg B/NH3 C
Oil and Grease (Soxhlet) SW846-9071B
Phenol (Colorimetric) SW846-9065
Phosphorus Adsorption Capacity MI DEQ
pH SW846-9045D
Solids, Total Suspended SM(20th)-2540D
Solids, Total SM(20th)-2540G
Solids, Volatile SM(20th)-2540G
SOUR (Specific Oxygen Uptake Rate, mg/g/hr) SM(20th)-2710B
Specific Gravity SM(20th)-2710F
Sulfide, Reactive SW846-7.3.4.2
Sulfide, Total SW846-9030B/9034
Volatile Acids Hach 8196
Volatile Solids Reduction (40-day VSR) SM(20th)-2540G
* Bacteria samples must be kept cool and delivered to the laboratory within 24 hours.
** BOD samples must be kept cool and delivered to the laboratory within 48 hours of sampling.

Individual Metals - ICP-OES

Metals Method
Sample Digestion SW846-3051
Aluminum SW846-6010B
Calcium SW846-6010B
Copper SW846-6010B
Iron SW846-6010B
Lithium SW846-6010B
Magnesium SW846-6010B
Manganese SW846-6010B
Molybdenum SW846-6010B
Phosphorus SW846-6010B
Potassium SW846-6010B
Silicon SW846-6010B
Silver SW846-6010B
Sodium SW846-6010B
Sulfur SW846-6010B
Zinc SW846-6010B

Individual Metals - ICP-MS

ICP-MS is not appropriate for all samples. We reserve the right to determine appropriate method and instrumentation.
Metals Method
Sample Digestion SW846-3051
Antimony SW846-6020
Arsenic SW846-6020
Barium SW846-6020
Beryllium SW846-6020
Boron SW846-6020
Cadmium SW846-6020
Chromium SW846-6020
Cobalt SW846-6020
Copper SW846-6020
Lead SW846-6020
Mercury SW846-6020
Molybdenum SW846-6020
Nickel SW846-6020
Selenium SW846-6020
Strontium SW846-6020
Thallium SW846-6020
Titanium SW846-6020
Vanadium SW846-6020
Zinc SW846-6020
Zirconium SW846-6020